Your Roll No.............. roree 

JAMIA HAMDARD 
School of Pharmacentical Education and Research 

M. Pharm. I Semester Examination (2023-24) 

niques Maximum Marks: 75 : Modern Pharmaceutical Analytieal T 

Paper Code: MPATOVT/MPRIOIT/MPCIOIT/ MPGLOIT/MPHIOIT/MPLIOIT /MQAIOIT 

Time: Three hours Date: 08-03-2024 

(Write your Roll No. on the top immediately on recelpt of this question paper) 

Note:  This paper has two Sections; A and B. 
Attempt all the two sections. 
Section A: Answer all the questions. — Section B: Answer any 4 out of 6 questions 

Abbreviations Used: 
CO-Course Outcome, I'O- Program Outcome, BTL- Bloom Taxonomy Level: BT level 1-Remember; BT level 2- 
Understand; BT level 3- Apply; BT level 4- Analyze; BT level 5- Evaluate; BT level 6- Create. 

SECTION-A 

Answer the following in bricf (Attempt all questions) 5x3= 15 Marks 

Q. No 1 [ Question BTL co ro 

(a) Describe the effects of conjugated double bonds in UV absorption bands 2 2 1 
of similar & different chromophores taking suitable examples 

(b) Describe the different types of vibrations that occur in the molecules on 3 2 2 
absorption of IR radiation 

() Describe Spin-Spin coupling and Coupling constants and their significance 1 2 2 
in NMR Spectroscopy 

(d) Describe the Principle of Potentiometry and its use in titrations. 2 2 2 

(¢) Describe the Principle and application of Differential Thermal Analysis | 2 2 
(DTA) 

SECTION B 

Long type Questions (Attempt any 4 out of 6) 4x15= 60 Marks 

S. No. Question BTL | CO [ PO 

Q. No2 Explain the difference in Principles of Flame Emission Spectroscopy and 2 2 3 
Atomic Absorpt cctroscopy. Describe in detail the instruments used in 
Atomic Absorption Spectroscopy with its applications. 

Q.No3 | Describe the Principles of FT-NMR, 13C-NMR Spectroscopy along with their 3 2 2 
applications. 

Q. Nod [ Explain the Principle of ctrophoresis, basic components of instruments, and 3 2 3 
factors affecting separation and applications. 

Q.No5 [ Describe the Rules for different pattems of Fragmentation in Mass 4 2 1 Spectrometry and their applications with respect to determination of Structure 
of Organic Molecules. 

Q-No6 | Describe the Principle of Chromatography, Classification, and applications of | 3 2 3 
different types of Chromatographic Techniques. 

Q.No7 [ Explain the Principle of FT-IR and its Applications in determining the structure | 3 2 3 
of Organic Molecules.